DEVELOPMENT AND MODELING OF CERAMIC WATER CANDLE FILTER FROM OHIA CLAY USING RESPONSE SURFACE METHODOLOGY

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Product Code: 00006819

No of Pages: 50

No of Chapters: 1-5

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ABSTRACT

The study aimed to optimize the production process of Ceramic candle filter by developing and modeling the ceramic filter using Response Surface Methdology (RSM). The development of model composing Ohiya Clay-Sawdust-Kaolin mix into varying qualities of ceramic candle filter products in accordance with end-user desires in other to attract investors in Abia State for economic growth in Nigeria. The effect of the input parameter such as; firing temperature, clay and sawdust ratio were studied. The result generally showed that the clay and sawdust has the greatest effect on the apparent porosity response. The result also revealed that 40:50:10 are the optimal mix of clay, sawdust and kaolin while the optimal firing temperature of ceramic candle is 900oc. While the performance test of the ceramic candle filter indicated a filtration efficiency of 78% and 79% for the total dissolved solid and total suspended solid respectively. The developed model can be used to predict apparent porosity for different firing temperatures and improve the efficiency of ceramic candle filters in water filtration. The study suggests that this method of production is cost-effective, efficient, and sustainable for water filtration.






TABLE OF CONTENTS

Title Page i
Declaration ii
Dedication iii
Certification iv
Acknowledgements v
Table of Contents vi
List of Tables ix
List of Figures x
List of Symbols and Abbreviation xii
Abstract xiv

CHAPTER 1: INTRODUCTION
1.1 Background of Study 1
1.2 Statement of Problem 2
1.3 Aim and Objectives of Study 3
1.4 Scope of Study 4
1.5 Justification for the Study 5

CHAPTER 2: LITERATURE RIVEW
2.1 Overview of Ceramic water filter 5
2.1.1 Types of Ceramic water filter 7
2.2 Properties of Ceramic candle water filter 8
2.3 Review of ceramic candle water filter 11

CHAPTER 3: MATERIALS AND METHODS
3.1 Materials 13
3.2 Methods 13
3.2.1 Body Preparation 15
3.2.2 Mixing 15
3.2.3 Slip Casting 15
3.2.3 Drying and Firing 16
3.3 Physical Analysis and Experimentation 17
3.3.1 Experimental Procedures 17
3.3.2 Making moisture Determination 17
3.3.3 Determination of Relative Plasticity 18
3.3.4 Determination of Modulus of Rapture 18
3.3.5 Shrinkage Determination 19
3.3.6 Determination of Water Absorption 19
3.3.7 Porosity and Density Determination 20
3.4 Response Surface Methodolgy 20
3.4.1 Application of RSM based Desirability Function Analysis 20

CHAPTER 4: RESULT AND DISCUSSION
4.1 Physical Analysis 22
4.1.1 Modulus of Rapture 25
4.2 Response Surface Modeling 27
4.2.1 Statistical Result 30
4.2.2 Residual Plots 32
4.2.3 Response Optimization 33

CHAPTER 5: CONCLUSION AND RECOMMENDATION
5.1 Conclusion 36
5.2 Recommendation 36
REFERENCE 
APPENDICE
 
 



LIST OF TABLLES

2.1 General strength and weakness of Ceramic water Candle filters 6

3.1 Formation of Candle filter bodies                                17

4.1 Results for water Absorption, Apparent porosity, Apparent Density      22

4.2 Total Linear Shrinkage 24

4.3 Modulus of Rapture 25

4.4 Experiment Design Table 27

4.5 Coded Coefficients 30

4.6 Model Summary 30

4.7 Analysis Summary 30

4.8 Response Optimization 30

4.9 Candle filter Performance Test 35
           




LIST OF FIGURES

3.1 Sample of Unprocessed Clay

3.1 Hardwood Sawdust

3.3 Water filtration setup using produce ceramic candle filter

4.1 Total and Linear Shrinkage Graph

4.3 Bar Chart for Modulus of Rapture

4.4 Parity plot of Predicted value versus actual (observed) value of Apparent porosity

4.5 Response Surface plot of Apparent porosity versus Sawdust and Clay

4.6     Pareto Chart of Standardized Effects

4.7 Residual Plot






CHAPTER 1
INTRODUCTION

1.1 BACKGROUND OF STUDY
The human body is said to be made up of about 70% water (Dang-I, A. Y. (2010). This shows how important water is to the survival of humans. The importance of water is such that life cannot be sustained beyond a few days, without it. Furthermore, the lack of adequate water supply leads to the spread of diseases. Water is used in most human domestic activities and most importantly for drinking, which is a means by which the water level in the human system is maintained. For domestic uses of water, the purity of water is very important, since it has a direct relationship with the health and well-being of the individual using the water (Guy J.B., (2003). 

In Nigeria, where efforts to improve people’s access to safe drinking water have been marred by social complexes, most of the rural areas and indeed appreciable parts of urban areas do not have access to quality potable drinking water. This usually gives rise to incessant epidemics killing thousands of infants and even adults. It is common knowledge that poverty-stricken rural communities are still dependent on unsafe drinking water containing a high rate of pathogens that cause epidemic gastrointestinal diseases (WWAP): Perugia, Italy, 2009). Ceramic filter has shown to be a veritable tool in water treatment as the materials are locally available while the method of production is simple. Despite the abundant raw materials for the production of candle filters for water filtration, candle filters are still imported into the country due to a lack of awareness and inadequate engineering equipment needed to explore candle filters production from local raw materials, making candle filters expensive beyond the reach of the average man. 

Filtration is the separation of solids from a suspension in a liquid by means of a porous medium or screen which retains the solids and allows the liquid to pass. In general, the pores of the medium are larger than the particles which are to be removed, and the filter works efficiently only after an initial deposit has been trapped in the medium (Coulson et.al (2002). Filtration technologies are adopted to remove unwanted contaminants, especially suspended solids from surface waters. Filtration has to do with the flow of water through a porous medium. The water is purified through a range of physical, chemical and biological mechanisms (Moshiri. G.A. (1993), et al(2005). Ceramic filtration is the use of porous ceramic to filter microbes and other contaminants from drinking water. The primary materials used in the manufacturing of ceramic candle filters are clay, combustible, and siliceous materials or grog a non-plastic material used to reduce shrinkage and control porosity. The combustible materials are used to increase the porosity of filter media by creating voids within the internal structure after the material has been sintered during firing. As a result, the goal of this project is to design and produce candle ceramic water filters using an ideal blend of Ohiya clay, grog, silica, and sawdust. In addition, the designed filter's performance effectiveness on performance parameters of water pH, total dissolved solids (TDS), and total suspended solids (TSS) of the sample after filtration was investigated.
 
1.2 STATEMENT OF THE PROBLEM
The problem being addressed in this research is the need for an effective and efficient water filtration method to combat water-borne diseases in developing countries. Despite the availability of various filtration methods, many communities continue to suffer from water-borne illnesses due to a lack of access to clean water and contamination from pollutants, water fetching and conveyance. To address this problem, this research aims to use response surface methodology (RSM) to optimize the design and performance of ceramic water filters as a solution to provide safe drinking water. The RSM will involve the collection and analysis of data on the effect of various input variables such as the properties of ceramic material, filter dimensions, and manufacturing process on the output variables such as filter's flow rate, filtration efficiency and pressure drop. The scope of the research will include laboratory testing and field studies to determine the optimal design, material and use of ceramic candle filters for this purpose by using RSM.

1.3 AIMS AND OBJECTIVES
The aim of this work is the development of ceramic water candle filter from Ohia clay for household water treatment using Response Surface Methodology (RSM). The specific objectives are:

i. Parametric evaluation of the influence of varying the ratio of Ohia clay and additives on the qualities of ceramic products developed from it using Response Surface Methodology(RSM)

ii. Develop a ceramic water candle filter that meets specific performance requirements such as flow rate, filtration efficiency, and pressure drop.

iii. Optimize the filter's design and performance by identifying the optimal combination of input variables using RSM.

iv. Determine the effect of various input variables on the output variables through experimentation and statistical analysis using RSM

v. Development of optimal formulation for producing a standard water candle filter.

1.4 SCOPE OF STUDY
This study was limited to the use of Ohiya clay for development of ceramic candle water filter. The process was designed and optimized using Response Surface Methodology 

1.5 JUSTIFICATION
Drinking water source contamination poses a great threat to human health in developing countries. Ceramic water filter treatment techniques, which improve drinking water quality at the household level, offer an affordable and convenient way to obtain safe drinking water and thus reduce the outbreaks of waterborne diseases. Ceramic water filters (CWFs), fabricated from locally sourced materials and manufactured by local labour, are one of the most socially acceptable water treatment technologies because of their effectiveness, low-cost and ease of use. Therefore, employing CWFs will be cost effective, eliminate importation, and improve employment through the local production of CWFs. The response surface modelling approach which will be employed in this study uses special experimental design with a small number of experimental runs to test the effect of several variables on all the responses involved at a time, which reduces the time and high cost of one-factor-at-a-time experimental approach (Kathleen et al. 2004). 


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