EFFECT OF METHANOL LEAF EXTRACT OF JATROPHA TANJORENSIS ON SOME CARDIAC FUNCTION BIOMARKERS IN ISOPRENALIN INDUCED MYOCARDIAL INFARCTION IN ALBINO RATS

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ABSTRACT

Coronary artery disease, and its end results myocardial infarction, is a significant cause of morbidity and mortality globally. Recently, there has been an increase in the incidence of myocardial infarction which manifests as a result of disrupted blood supply and oxygen to the myocardium. This present study evaluated the effect of methanol leaf extract of Jatropha tanjorensis on some cardiac function biomarkers in isoprenaline-induced myocardial infarction in albino rats. The in vitro qualitative phytochemical and antioxidant properties of Jatropha tanjorensis leaves were determined using standard analytical methods. Thirty six (36) albino rats were used for the in vivo study and randomly divided into six (6) groups of six rats per group. Group 1 served as the normal control, group 2 was the negative control (administered 85mg/kg of isoprenaline only), group 3 served as the positive control (pretreated with 2mg/kg carvedilol for 28 days), groups 4, 5 and 6 were pretreated with 200, 400 and 600mg/kg of methanol leaf extract of Jatropha tanjorensis respectively, for 28 days. Myocardial infarction was induced in the rats using subcutaneous injection of 85mg/kg isoprenaline (ISO) for two consecutive days (26th and 27th) at 24 hours intervals. The in vitro phytochemical and antioxidant results revealed that Jatropha tanjorensis leaves possess good bioactive compounds such as alkaloids, terpenoids, flavonoids, steroids, tannins, saponins, phenolics and free radical scavenging potency. The acute toxicity study of the extract recorded no death even at the high dose of 5000mg/kg. The result of the in vivo study showed that isoprenaline effectively induced myocardial infarction in rats, reflected by the  significant (p<0.05) increases, in the negative control group, of the measured biomarkers  (Creatine Kinase-MB activity, Troponin I activity, Lactate Dehydrogenase acitivity, Aspartate aminotransferase activity, Alanine aminotransferase activity, high sensitivity C-Reacting Protein concentration, Triacyglycerol concentration, Cholesterol concentration and Malondialdehyde concentration) relative to the normal control. The extract (400mg/kg) significantly (p<0.05) decrease CK-MB activity, Troponin I activity, LDH acitivity, AST activity, ALT activity, hsCRP concentration, TAG concentration, Cholesterol concentration, and MDA concentration while increasing HDL concentration, catalase activity, SOD activity, GPx activity and GSH concentration. The histopathological study showed different degrees of cardiac alteration. There was marked histomorphological alteration, severe widespread myocardial necrosis of the heart, atrophy of hepatic cord but mild multifocal vascuole degeneration of the renal tubular epithelial lining cell in the group administered 600mg/kg of the extract and the negative control compared to the normal control. This indicated that the extract at 600mg/kg dose does not possess cardioprotective potency. The carvedilol at 2mg/kg dose showed moderate potency in restoring damage cells. The methanol leaf extract of Jatropha tanjorensis at moderate dose (400mg/kg) attenuated the effect of isoprenaline-induced myocardila damage without alteration of the liver and kidney. This study suggested that the extract to some extent could serve as an agent for the prevention of cardiotoxicity.




TABLE OF CONTENTS

Title page                                                                                                                                                                                                        i

Declaration                                                                                                                                                                                                      ii

Certification                                                                                                                                                                                        iii

Dedication                                                                                                                                                                                                      iv

Acknowledgement                                                                                                                                                                              v

Table of Contents                                                                                                                                                                               vi

List of Tables                                                                                                                                                                                      xiii

List of Figures                                                                                                                                                                                     xiv

List of Plates                                                                                                                                                                                       xv

Abstract                                                                                                                                                                                                          xvii

CHAPTER 1:            INTRODUCTION

1.1                   Background of the Study                                                                                                                                           1

1.2                   Statement of the Problem                                                                                                                               3

1.3                   Aim and Objectives of the Study                                                                                                                   4

1.3.1    Aim of the study                                                                                                                                                                     4

1.3.2    Objectives of the research                                                                                                                                           4

1.4                   Justification for the study                                                                                                                                           5

CHAPTER 2:            LITERATURE REVIEW

2.1                   Myocardial Infarction                                                                                                                                     6

2.1.1    Signs and symptoms of myocardial infarction                                                                                   6

2.1.2    Causes of myocardial infarction                                                                                                                     7

2.1.3    Mechanism of myocardial infarction                                                                                                  8

2.1.4    Types of myocardial infarction                                                                                                                       8

2.1.4.1 ST- elevation myocardial infarction (STEMI)                                                                                    9

2.1.4.2`            Non-ST elevation myocardial infarction (NSTEMI)                                                              9

2.1.4.3 Unstable angina                                                                                                                                                                      9

2.1.4.4 Myocardial infarction type 1                                                                                                                          9

2.1.4.5 Myocardial infarction type 2                                                                                                                          10

2.1.4.6 Myocardial infarction type 3                                                                                                                          12

2.1.4.7 Myocardial infarction type 4a                                                                                                                         12

2.1.4.8 Myocardial infarction type 4b                                                                                                                        12

2.1.4.8 Myocardial infarction type 4c                                                                                                                         13

2.1.4.9 Myocardial infarction type 5                                                                                                                          13

2.2                   Biomarkers for Evaluation of Myocardial Infarction                                                             13

2.2.1    Creatinine kinase MB (CK-MB)                                                                                                                     14

2.2.2    Troponin                                                                                                                                                                                  14

2.2.3    Aspartate amino transferase (AST)                                                                                                                 14

2.2.4    Lactate dehydrogenase (LDH)                                                                                                                                   15

2.2.5    Heart fatty acid‑binding protein (H‑FABP).                                                                          15

2.2.6    Myoglobin:                                                                                                                                                                              15

2.3                   Incidence and Prevalence of Myocardial Infarction                                                              16

2.4                   Diagnosis and Management of Myocardial Infarction.                                                          17

2.5                   Free Radicals and Oxidative Stress                                                                                                                18

2.5.1    Mechanism of reaction of free radicals and oxidative stress                                      18

2.6                   Role of Oxidative Stress in Cardiovascular Diseases                                                             19

2.6.1    Oxidative stress and hypertension                                                                                                                  19

2.6.2    Oxidative stress and heart failure                                                                                                                   20

2.6.3    Oxidative stress and myocardial ischemia reperfusion injury                                     21

2.7                   Overview of Jatropha tanjorensis                                                                                                                  23

2.8                   Pharmacological Properties of Jatropha tanjorensis                                                               24

2.8.1    Hepatoprotective effect                                                                                                                                              24

2.8.2    Antioxidant                                                                                                                                                                             24

2.8.3    Antidiabetic effect                                                                                                                                                      24

2.8.4    Anticancer effect                                                                                                                                                       24

2.8.5    Antianaemic effect                                                                                                                                                     25

2.8.6    Anti-ulcer effect                                                                                                                                                                     25

2.8.7    Phytoconstituent of Jatropha tanjorensis                                                                                           25

2.8.8    Hypolipidemic activity                                                                                                                                               26

2.8.9    Antibacterial effect                                                                                                                                                     26

2.9                   Cardioprotective Properties of Some Medicinal Plants                                                          26

2.9.1    Moringa plant                                                                                                                                                             26

2.9.2    Vernonia amygdalina                                                                                                                                                  27

2.9.4    Garcinia kola                                                                                                                                                              28

2.9.5    Anarcadium occidentale                                                                                                                                             28

2.9.6    Mucuna puriens                                                                                                                                                                      29

2.9.7    Zingiber officinale                                                                                                                                                       30

2.9.8    Allium sativum                                                                                                                                                            30

2.9.9    Allium cepa                                                                                                                                                                             31

2.9.10  Curcuma longa                                                                                                                                                                       32

2.9.11  Hibscus sabdariffa                                                                                                                                                      33

CHAPTER 3:            MATERIALS AND METHODS

3.1                   Materials                                                                                                                                                                                 34

3.1.1    Collection of plant leaves                                                                                                                                           34

3.1.2    Chemicals/reagents used                                                                                                                                             34

3.2                   Methods                                                                                                                                                                                  34

3.2.1    Extract preparation                                                                                                                                                     34

3.2.2    Phytochemical screening                                                                                                                                             35

 3.2.2.1            Test for alkaloids                                                                                                                                                        35

3.2.2.2 Test for steroids                                                                                                                                                                      35

3.2.2.3 Test for flavonoids                                                                                                                                                      35

3.2.2.4 Test for tannins                                                                                                                                                                       35

3.2.2.5 Test for saponins                                                                                                                                                         35

3.2.2.6 Test for terpenoids                                                                                                                                                      36

2.2.2.7 Test for phenolics                                                                                                                                                        36

2.2.3    In Vitro Antioxidants                                                                                                                                                  36

3.2.3.1 Determination of total phenol content                                                                                                            36

3.2.3.2 Determination of total flavonoid content                                                                                           37

3.2.3.3 Determination of hydrogen peroxide scavenging capacity                                        37

3.2.3.4 Determination of reducing power                                                                                                                   38

3.2.3.5 Determination of nitric oxide (NO) scavenging activity                                                        38

3.2.3.6 Determination of lipid peroxidation assay                                                                                          39

3.2.4    Experimental animals                                                                                                                                      39

3.2.5    Acute toxicity test (LD50)                                                                                                                                           39

3.2.6    Experimental design                                                                                                                                                   40

3.2.7    Biochemical estimations                                                                                                                                             41

3.2.7.1 Assay of alanine amino transferase (ALT) activity                                                                41

3.2.7.2 Assay of serum aspartate aminotransferase (AST) activity                                        42

3.2.7.3 Lactate dehydrogenase (LDH) activity                                                                                                          43

3.2.7.4 Determination of CK-MB activity                                                                                                     43

3.2.7.5 Determination of high sensitivity c-reactive protein (hsCRP)                                    44

3.2.7.6 Determination of troponin level:                                                                                                                     46

3.2.8    Antioxidant estimation in serum                                                                                                                     47

3.2.8.1 Estimation of extent of lipid peroxidation                                                                                         47

3.2.8.2 Assay of superoxide dismutase activity                                                                                                         48

3.2.8.3             Assay for catalase activity                                                                                                                              48

3.2.8.4 Estimation of glutathione peroxidase activity                                                                                    49

3.2.8.5 Reduced glutathione estimation                                                                                                                     50

3.2.9    Lipid profile tests                                                                                                                                                        51

3.2.9.1 Determination of serum total cholesterol                                                                                            51

3.2.9.2 Determination of serum triacylglycerol concentration                                                            52

3.2.9.3 Determination of serum high density lipoprotein-cholesterol concentration54

3.2.10  Organ weight to body weight ratio                                                                                                                55

3.2.11  Histopathological examination                                                                                                                       55

3.2.11.1           Tissue preparation                                                                                                                                                       55

3.2.11.2           Slide examination                                                                                                                                                       56

3.3                   Statistical analysis                                                                                                                                                       56


CHAPTER 4:            RESULTS AND DISCUSSION

4.1                   Results                                                                                                                                                                                    57

4.1.1:   Phytochemicals present in methanol extract of Jatropha tanjorensis leaves57

4.1.2:   Total (phenols and flavonoids) content and in vitro IC50 values of

antioxidants                                                                                                                                                                   58

 

4.1.3    Reducing power of Jatroph tanjorensis.                                                                                             59

4.1.4:   Nitric oxide (NO) scavenging ability of Jatropha tanjorensis                                    60

4.1.5:   Hydrogen peroxide (H2O2) scavenging ability of Jatropha tanjorensis         61

 

4.1.6:   Lipid peroxidation ability of Jatropha tanjorensis.                                                                62

 

4.1.7:  Acute toxicity study of methanol extract of Jatropha tanjorensis leaves       63

 

4.1.8:     Effect of methanol leaf extract of Jatropha tanjorensis on body weight and organ weights                                                                                                                                                                    64

4.1.9:   Effect of methanol leaf extract of Jatropha tanjorensis on serum troponin

activity                                                                                                                                                                                       65

 

4.1.10: Effect of methanol leaf extract of Jatropha tanjorensis on serum CK-MB

activity                                                                                                                                                                                       66

 

4.1.11: Effect of methanol leaf extract of Jatropha tanjorensis on serum LDH

activity                                                                                                                                                                                       67

 

4.1.12: Effect of methanol leaf extract of Jatropha tanjorensis on serum hsCRP

concentration.                                                                                                                                                                68

 

4.1.13: Effect of methanol leaf extract of Jatropha tanjorensis on serum AST

concentration.                                                                                                                                                                69

 

4.1.14: Effect of methanol leaf extract of Jatropha tanjorensis on serum ALT

concentration.                                                                                                                                                                70

 

4.1.15: Effect of methanol leaf extract of Jatropha tanjorensis on serum TAG

                        concentration.                                                                                                                                                             71

 

4.1.16: Effect of methanol leaf extract of Jatropha tanjorensis on serum

total cholesterol concentration.                                                                                                              72

 

4.1.17: Effect of methanol leaf extract of Jatropha tanjorensis on serum HDL

concentration.                                                                                                                                                                73

 

4.1.18: Effect of methanol leaf extract of Jatropha tanjorensis on serum SOD

activity.                                                                                                                                                                                      74

 

4.1.19: Effect of methanol leaf extract of Jatropha tanjorensis on serum GPx

activity.                                                                                                                                                                                      75

 

4.1.20: Effect of methanol leaf extract of Jatropha tanjorensis on serum glutathione

concentration.                                                                                                                                                                76

 

4.1.21: Effect of methanol leaf extract of Jatropha tanjorensis on serum catalase

activity.                                                                                                                                                                                      77

 

4.1.22: Effect of methanol leaf extract of Jatropha tanjorensis on serum MDA

concentration.                                                                                                                                                                78

 

4.1.23: Histopathological analysis                                                                                                                              79

4.2                   Discussion                                                                                                                                                                               85

CHAPTER 5:            CONCLUSION AND RECOMMENDATIONS

5.1                   Conclusion                                                                                                                                                                              93

5.2                   Recommendation                                                                                                                                                        94

References                                                                                                                                                                                

Appendices

 

 




 

LIST OF TABLES

                                                                                                                                                                                                                        PAGE

4.1                   Phytochemicals present in methanol extract of Jatropha tanjorensis leaves 57

4.2:      Total (phenols and flavonoids) content and in vitro IC50 values of

antioxidants                                                                                                                                                                   58

 

4.3:      Acute Toxicity Study of methanol extract of Jatropha tanjorensis leaves    63

4.4:        Effect of methanol leaf extract of Jatropha tanjorensis on body weight and organ weights                                                                                                                                                                    64

 

 

 

 

 

 

LIST OF FIGURES

                                                                                                                                                                                                                        PAGE

4.1                   Reducing power of Jatroph tanjorensis.                                                                                             59

4.2:      Nitric oxide (NO) scavenging ability of Jatropha tanjorensis                                    60

 

4.3:      Hydrogen Peroxide (H2O2) scavenging ability of Jatropha tanjorensis         61

 

4.4:      Lipid peroxidation ability of Jatropha tanjorensis.                                                                62

 

4.5       :           Effect of methanol leaf extract of Jatropha tanjorensis on serum troponin

activity                                                                                                                                                                                       65

 

4.6:                  Effect of methanol leaf extract of Jatropha tanjorensis on serum CK-MB

Activity.                                                                                                                                                                         66

 

4.7:                  Effect of methanol leaf extract of Jatropha tanjorensis on serum

LDH activity                                                                                                                                                                  67

 

4.8:                  Effect of methanol leaf extract of Jatropha tanjorensis on serum

hsCRP concentration                                                                                                                                         68

 

4.9:                  Effect of methanol leaf extract of Jatropha tanjorensis on serum

AST concentration.                                                                                                                                            69

 

4.10:    Effect of methanol leaf extract of Jatropha tanjorensis on serum ALT

Concentration.                                                                                                                                                               70

 

4.11:    Effect of methanol leaf extract of Jatropha tanjorensis on serum TAG

concentration                                                                                                                                                                 71

 

4.12:    Effect of methanol leaf extract of Jatropha tanjorensis on serum total

cholesterol concentration                                                                                                                                   72

 

4.13:    Effect of methanol leaf extract of Jatropha tanjorensis on serum HDL

Concentration.                                                                                                                                                               73

 

4.14:    Effect of methanol leaf extract of Jatropha tanjorensis on serum SOD

activity                                                                                                                                                                                       74

 

4.15:    Effect of methanol leaf extract of Jatropha tanjorensis on serum GPx

activity                                                                                                                                                                                       75

 

4.16:    Effect of methanol leaf extract of Jatropha tanjorensis on serum

glutathione concentration                                                                                                                      76

 

4.17:    Result on the effect of methanol leaf extract of Jatropha tanjorensis on

serum catalase activity                                                                                                                                       77

 

4.18:    Effect of methanol leaf extract of Jatropha tanjorensis on serum MDA

Concentration.                                                                                                                                                               78

 

 


 

 

 

 

LIST OF PLATES

                                                                                                                                                                                                                        PAGE

A-C                 Sections of the heart, liver and kidney from normal (control) rats                             80

 

A-C:    Sections of the heart, liver and kidney from rats given distilled

water and isoprenaline (85mg/kg)                                                                                                          81

 

A-D:    Sections of the heart from the pretreated groups                                                                   82

 

A-D:    Sections of the liver from the pretreated groups                                                                                83

 

A-D:    Sections of the kidney from the pretreated groups                                                                84

 

 

 

 


 

 


 

CHAPTER 1

INTRODUCTION


1.1       BACKGROUND OF THE STUDY

Globally, there is increase in the number of deaths resulting from the generation of free radicals and oxidative stress. Metabolic pathways and environmental pollution easily generate free radicals which are also regarded as reactive species (Souri et al., 2008; Neha and Lubna, 2014). Different factors can elevate and accumulate the level of oxidative stress and free radicals which easily prevent the cell from working effectively. This can then lead to damage of cells, and has main contributory role in pathogenesis of cardiovascular diseases (Mohanty et al., 2007; Mahammad et al., 2012).

According to the American Heart Association and World Health Organization statistics, cardiovascular diseases (CVDs) are regarded as the main cause of death worldwide (Mozaffarian et al., 2016). CVD mostly refers to MI (Myocardial infarction), angina pectoris, hypertension, stroke and other circulatory diseases. Coronary artery diseases, congestive heart failure, cardiac arrest, arrhythmias, and peripheral artery diseases are the most commonly reported heart diseases (Mallapu et al., 2017).

A coronary artery disease which is also called Ischemic heart disease is a crucial problem worldwide and is known as major non transmissible disease (Abubaker et al., 2012). A good example of ischemic heart disease is acute myocardial infarction (MI) and it manifest due to inequality between coronary blood supply and myocardial demand. Myocardial damage due to free radicals is an imperative etiological mechanism that is linked with increased level of reactive oxygen species and/or insufficient antioxidant defense system (Geeta et al., 2016). Isoprenaline (ISO) is a synthetic catecholamine with active effect on non-selective beta-adrenergic agonist and low affinity for alpha adrenergic receptors. It has the tendency to produce myocardial lesions and cell death at high doses. Various drugs with cardioprotective effects such as bisoprolol, metoprolol, carvedilol and timolol have been studied using isoprenaline-induced myocardial infarction model. However the adverse effect associated with modern medicines have limited their effective used in preventing heart diseases (Upaganlawar et al., 2011).

Leafy vegetables play vital role in the food culture of many African households and it is part of Africans’ cultural heritage (Mensah et al., 2008; Omoregie et al., 2011). Nigeria is blessed with a multiplicity of indigenous green leafy vegetables which are consumed by various groups for different purpose (Omoregie et al., 2011). Medicinal plants are unique in their ability to treat several human ailments because they contain various valuable phytoconstituents. Secondary plant metabolites such as steroids, alkaloids, flavonoids, glycosides, terpenoids, tannins, saponins, phenolic compounds etc. are mainly accountable for the healing potency of the plant (Omoregie et al., 2011).

Medicinal plants have been used for centuries to combat many health challenges and are also useful component in pharmaceutical industries; among these leafy vegetables is Jatropha tanjorensis. Jatropha tanjorensis known as Chaya leaf and generally known as ‘Hospital too far’ in Nigeria is a shrub from the family Euphorbiaceae. Different parts of Jatropha plants are used in many ways and in different countries.

Jatropha tanjorensis leaves have been reported to possess numerous medicinal properties such as hepatoprotective (Ezeonu et al., 2017; Madubuike et al., 2015), antidiabetic (Momoh et al., 2014; Chinenye et al., 2019), anticancer (Purshothaman et al., 2014), antianaemic (Ameloko 2010; MacDonald et al., 2014), antiulcer (Epison et al., 2016), hypolipidemic (Oyewole and Akingbala, 2011; Ijioma et al., 2014), antioxidant (Omoregie et al., 2011), antibacterial (Oboh and Masodje, 2009; Daniyan et al., 2018) among others.


1.2       STATEMENT OF THE PROBLEM

The Prevalence of myocardial infarction as the leading cause of death worldwide is a public health challenge. Myocardial infarction is a disorder in which there is myocardial cell necrosis due to substantial and persistent ischaemia. It is usually, but not always an acute manifestation of atherosclerosis-related coronary heart diseases, which implies obstructing mechanisms (Mendis, et al., 2011). The most prominent causes of myocardial infarction are ischemic heart disease/coronary artery disease resulting from an obstruction in blood flow leading to an inequality in myocardial oxygen supply (Mulqueen, 2015). Atherosclerotic disease generally accepted as coronary artery disease can lead to sudden formation of a blood clot on top of plaque that reduces blood flow in an already narrowed vessel (Steinbaum, 2017; Cleaveland, 2019).

There is a link between inflammation and evolution of heart attack. The inflammation of the coronary artery walls over time increases the accumulation of fatty plaques.  Several cardiovascular disease risk factors can result to the manifestation of myocardial infarction. Cardiovascular disease (CVD) is regarded as the major cause of mortality and disability in advanced countries (Mozaffarian et al., 2016).  Further, the frequent rise in common risk factors for CVD and the metabolic syndrome, have necessitated the search for more effective approaches to prevent and treat these cardiometabolic disorders (Koren et al., 2011). Consumption of natural antioxidants has been reported to contribute in the reduction of cardiovascular disease. Plants, herbs and spices rich in phenolic compounds are known to have pharmacological activities which can be traced to their antioxidant properties (Ashok-kumar et al., 2008; Madubuike et al., 2015).

Many studies have reported the antioxidant, anti-inflammatory, antibiotic, antihypertensive, antispasmodic, antiulcer, hypoglycemic and hypocholesterolemic activities of Jatropha tanjorensis (Bais et al., 2014).

Been that very few publications have been reported about the myocardial beneficial effect of Jatropha tanjorensis, the present study will evaluate whether Jatropha tanjorensis leaves extract has cardioprotective effect against ischemic myocardial infarct model in albino rats.


1.3       AIM AND OBJECTIVES OF THE STUDY

1.3.1    Aim of the study

The aim of this study was to evaluate the effect of methanol leaf extract of Jatropha tanjorensis on some cardiac function biomarkers in isoprenaline induced myocardial infarction in albino rats.


1.3.2    Objectives of the study

The objectives of this study were:

(i)                 To determine qualitative phytochemical constituents of the plant extract.

(ii)               To determine the in-vitro and in vivo (superoxide dismutase, catalase, glutathione peroxidase, reduced glutathione and MDA) antioxidant properties of Jatropha tanjorensis leaf.

(iii)             To determine the median lethal dose (LD50) of the methanol extract of Jatropha tanjorensis leaf.

(iv)             To determine the effects of the methanol leaf extract of Jatropha tanjorensis on some cardiac biomarkers (Troponin I, Creatine kinase-MB, LDH, AST, ALT, hsCRP) activity in albino rats.

(v)               To determine the effects of the methanol leaf extract of Jatropha tanjorensis on some lipid profile (TAG, HDL, Cholesterol) concentration in albino rats.

(vi)             To carry out histological studies on the heart, liver and kidney of the experiment animals


1.4       JUSTIFICATION FOR THE STUDY

The present investigation is a continuation of the research efforts aimed at providing the requisite scientific information and empirical data on the therapeutic value, toxicological potential and active principles of Nigerian medicinal plants as used in the management and treatment of several ailments. Jatropha tanjorensis leaf has recently received a lot of attention for both its nutritional and antioxidant properties and several researchers have shown that Jatropha tanjorensis possesses hypoglycemic, hypolipodermic, antioxidant and antimicrobial properties among others. The present study is designed to validate the ethnomedicinal use of Jatropha tanjorensis leaves using methanol as the solvent for extraction. This will also serve as a basis to recommend the continuous use of the plant in ethnopharmacology.


 

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