DETERMINATION OF CYANIDE CONTENT IN YELLOW ROOT AND WHITE ROOT CASSAVA TUBER (MANIHOT ESCULANTA CRANTZ) FROM NATIONAL ROOT CROP RESEARCH INSTITUTE, UMUDIKE

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Product Code: 00007342

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ABSTRACT


The Cyanide Content of four varieties of Cassava: (Tropical Manihot Selection; TMS 01/1638), (Tropical Manihot Selection; TMS 01/1412), (Tropical Manihot Selection; TMS 419), and (Tropical Manihot Selection; TMS 98/0505), from National Root Crop Research Institute (NRCRI), Umudike were studied using Picrate method. The Cyanide contents were: TMS 01/1638 (0.424 ) mg/kg, TMS 01/1412 (0.443 ) mg/kg, TMS 419 (0.557 ), AND TMS 98/0505 (0.518 ) mg/kg. The Cyanide content of the Yellow Root Cassava was found to be low compared to the White Root Cassava. The results of the Cyanide Content in the Current study were found to be within the acceptable unit as recommended by WHO.





TABLE OF CONTENTS

Cover Page                                                                                                                             

Title Page                                                                                                                                i

Declaration                                                                                                                              ii

Dedication                                                                                                                              iii

Certification                                                                                                                            iv

Acknowledgements                                                                                                                v

Table of Contents                                                                                                                   vi

List of Figures                                                                                                                         ix

List of Tables                                                                                                                          x

Abstract                                                                                                                                  xi

 

CHAPTER 1: INTRODUCTION

1.1       Background of the Study                                                                                           1

1.2       Statement of the Problem                                                                                           3

1.3       Aims and Objectives of the Study                                                                             4

1.4       Significant of the Study                                                                                             4

1.5       Scope of the Study                                                                                                     5

 

CHAPTER 2: REVIEW OF RELATED LITERATURE

2.1       Cassava Plant (Manihot esculenta crantz)                                                                   6

2.1.1    History of the cassava plant                                                                                        7

2.1.2    Production/economic impact of cassava                                                                     7

2.2       Cassava Toxicity                                                                                                         8

2.3       Cassava Products and Varieties                                                                                  9

2.3.1    Fermentation of cassava and its products                                                                   9

2.4       Cyanide                                                                                                                       10

2.4.1    History of cyanide                                                                                                      11

2.4.2    Forms of cyanide                                                                                                        11

2.5       Sources of Cyanide                                                                                                     14

2.5.1    Production and synthesis of cyanide                                                                          14

2.5.2    Application and uses of cyanide                                                                                 15

2.5.3    Cyanide Poisoning                                                                                                      16

 

2.5.4    Effect of cyanide poisoning                                                                                       17

2.5.5    Cyanide poisoning detection                                                                                      17

2.5.6    Cyanide poisoning treatment                                                                                      18

2.5.7    Cyanide irreversible toxicity and inhibition                                                                19

2.5.8    Toxicity of cyanide                                                                                                     19

2.5.8.1 Acute toxicity                                                                                                             20

2.5.8.2 Mechanism of acute cyanide poisoning                                                                      20

2.5.8.3 Chronic toxicity                                                                                                          21

2.5.8.4 Neurological effects                                                                                                    21

2.5.8.5 Tropical ataxic neuropathy (TAN)                                                                              22

2.5.8.6 Konzo                                                                                                                         22

2.5.9    Technique analysis of cyanide reduction                                                                    23

2.5.10  Removal of cyanide constraints from cassava                                                            23

2.6       Enzyme Inhibition                                                                                                      24

2.6.1    Form of inhibition                                                                                                       24

 

CHAPTER 3: MATERIALS AND METHODS

3.1       Sample Collection                                                                                                       30

3.2       Sample Preparation                                                                                                     30

3.3       Methods                                                                                                                      30

3.3.1    Preparation of alkaline picrate solution                                                                       31

3.3.2    Preparation of the stock solution for the concentration                                              31

3.4       Determination of Cyanide Content                                                                            31

 

CHAPTER 4: RESULTS AND DISCUSSION

4.1       Results                                                                                                                        34

4.2       Discussion                                                                                                                   39

 

CHAPTER 5: CONCLUSIO N AND RECOMMENDATION

5.1       Conclusion                                                                                                                  40

5.2       Recommendation                                                                                                        41

References                                                                                                                 42

 

 

 

  

 

LIST OF FIGURES

Figure

4.1       Absorbance reading of the Samples                                                                           33

4.2       Diluted Samples with 100 ml of Distilled Water                                                       34

4.3       Not Diluted Samples with 100 ml of Distilled Water                                                            34

 

 

 

 

 

LIST OF TABLES

Table

4.1       Absorbance Reading of the Diluted Stock Solution                                                  31

4.2       Absorbance Reading of the Non-Diluted Stock Solution                                          32

4.3       Results of Cyanide Content                                                                                       33

4.4       Results of Diluted Sample with 100 ml of Distilled Water                                        34

4.5       Results of Non-Diluted Sample with 100 ml of Distilled Water                               35

 

 

 


 

 

CHAPTER 1

INTRODUCTION


1.1              BACKGROUND OF THE STUDY

Cyanide, a toxic contaminant, occurs naturally in most plants but has high concentration in cassava and bamboo shoot. It is released into the environment through volcanoes and natural biogenic processes from higher plants, bacteria, algae and fungi (ATSDR, 1997) burning biomass, discharges from industries, waste water, tobacco smoke, wood smoke, smoke from burning plastics, vehicular emission, inadequately processed cassava products e.t.c (ATSDR, 1997). Exposure to small amounts of cyanide can be deadly regardless of the route of exposure. Cyanide is very poisonous, it stops cellular respiration by inhibiting an enzyme in mitochondria called cytochrome c. oxidase in the body.

Various poisonous substances that affect human metabolism have been identified in some edible plants. One of such poisonous substances is linamarin, a cyanogenic substance that is highly concentrated in cassava (Gari, 2002). Cassava (Manihot escilanta, crantz) constitutes one of the major stable foods for an estimated 500 million people in the tropical world and 700 million people worldwide (Kaur et al., 2009). The high carbohydrate content makes cassava a major food item especially for the low income earners in most tropical countries especially Africa and Asia (Li et al., 2001). The main food source is the starchy roots while the leaves are processed and used as sources ofprotein in Africa (ATSDR, 1997). The tubers are processed into gari, fufu, chips and flour for baking bread and biscuits (Robert et al., 2000). Thus, cassava serves as a major source of dietary energy but deficient in protein (Ano et al., 2007).

Nigeria ranked first among major producers of cassava in the world, producing about 33 million metric tons of cassava in 1993 (Ugwu et al., 2011). Over 95% of cassava produced in Nigeria is used as food for the country’s teeming population, being one of the countries staple foods (Alloway, 1995). However, the presence of cyanogenic glycosides (linamarin) in cassava has greatly affected utilization of cassava as food source. The cyanogenic glycosides form effective biological system to deter predators (Ugwu et al., 2011). Cyanide binds to the enzyme, cytochrome oxidase which negatively affects respiration. Akintonwa et al., (1994) had earlier reported cases of consuming cassava diets containing high levels of dietary cyanide. Non-fatal doses of cyanide have been associated with such symptoms like dizziness, headache, stomach pains, vomiting and diarrhea which appear four or more hours after consuming poorly processed cassava. In some cases, excessive consumption of cassava due to improper preparation has been linked to such ailments like goiter, ataxia (a neurological disorder affecting the ability to walk) (Pope et al., 2001), chronic pancreatitis (Hahn and Keyser, 1985) and even death. Toxic levels of cyanogenic glycosides have been used as the basis for categorizing cassava varieties. The less toxic varieties are designated as sweet cassava (Manihot palmate) while the more toxic varieties are designated as bitter cassava (Manihot utilissima). The bitter variety is widely cultivated because of its high yield and economy although, has high concentration of cyanogenic glycoside (100-500 mg/kg fresh weight), and is distributed throughout the tuber. The sweet variety has low concentration of

cyanogenic glycoside (less than 100 mg/kg) which is confined mostly to the peels (Philips, 1983). Cyanide level of less than 50 mg/kg is slightly poisonous, 80-100 mg/kg is toxic and levels above 100 mg/kg are fatal especially in grated cassava (Stone, 2002). In most cases, the cyanogens in fresh cassava roots are detoxified during processing into edible products (Wyllie et al., 1984). The processing of cassava roots commences with the peeling of the tubers, which contains higher cyanide content than the pulp. Removal of the peels therefore reduces the cyanogenic glycoside content considerably (Tewe, 1983). Thus, the selection of cassava species to be grown is very important. This study aimed at determining the cyanide content of varieties of cassava grown in NRCRI Umudike, of Abia State, Nigeria. This will assist farmers in their choice of cassava for cultivation.

 

1.2              STATEMENT OF THE PROBLEM

Cassava (Manihot esculenta crantz) is a staple food in most tropical regions, and is grown over a range of climates and altitudes and on a wide variety of soils. The estimated total world cassava production in 2012 was 256 million tonnes according to FAO (2013), which is an increase of 40% since 2000. Africa represents the continent with the largest cassava production of more than

50% of the annual world production. The crop is one of the most important staple food with about 93% of the production used for human consumption (Nweke et al., 2002). The roots of this important carbohydrate source are eaten both fresh and as processed products (Westby, 2002). However, in its tissue, cassava contains cyanogenic glycosides, mainly linamarin, that are enzymatically hydrolysed to glucose, acetone and hydrogen cyanide during cell rupture (Conn, 1994). The released cyanide is highly toxic for humans and is a threat to the cassava consumer (Rosling, 1988). The presence of cyanogenic glycosides in cassava tissues is related to illnesses that occur in populations where cassava is the staple food. These illnesses include tropical ataxic neuropathy, epidemic spastic paraparesis, also known as konzo (Cliff et al., 2011). These problems have been reported in the Democratic Republic of Congo, Nigeria, Tanzania and Mozambique (Ciglenecki et al., 2011).

 

1.3    AIM AND OBJECTIVES OF THE STUDY

The major aim of this research work is to determine the cyanide content in yellow root and white root cassava tuber (Manihot esculanta, crantz).

The specific objectives of this research work are outlined as follows:

1.      To determine the cyanide content of the cassava varieties in the study area

2.      To determine the of level of Cyanide of released new cassava varieties in breeding programs in the study area.

 

1.4              SIGNIFICANCE OF THE STUDY

Due to the evidence of the toxicity of cassava, it is of utmost importance to ascertain the level of cyanide present in cassava varieties in the study area especially in new varieties of cassava programs bread at NRCRI.

  

1.5              SCOPE OF THE STUDY

This study is limited to the analysis of cyanide content of different varieties of cassava bread at National Root Crops Research Institute Umudike in Abia state.

 

 

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